Archive for the ‘Chemistry’ Category

Vapor Deposition of Carbon Nanotubes

Wednesday, March 2nd, 2011

The unique chemical and physical properties of carbon nanotubes (CNTs), which make them suitable for a wide range of applications, have stimulated interest for research since their discovery.

Among the developed methods for growing CNTs, the catalytic chemical vapor deposition (CCVD) of hydrocarbon gases turns out to be very promising because of its comparative simplicity, ease of control and low cost. (more…)

Reflection and Transmission of Chlorine Content Color Wheel

Wednesday, February 2nd, 2011

Background

The customer supplied us with a special wheel used for chlorine content measurements.  The provided sample has nine windows of varying shades of yellow, with a clear center window for reference, as shown in Figure 1.  (more…)

Raman Analysis of Pharmaceutical Ingredients

Thursday, September 2nd, 2010

A range of options is available for Raman analysis, including systems suitable for handheld, laboratory and educational applications. Systems typically include a spectrometer, laser, operating software and sampling accessories, while modular options are available for users to configure their own Raman systems. Most applications are handled in the 150-3200 cm-1 range, with resolution of ~6-10 cm-1. (more…)

Effect of Sandblasting on the Specular Reflection from Encoder Wheels

Friday, July 16th, 2010

Goal:
Determine the impact of sandblasting on specular reflection from different types of encoder wheels

Experimental Conditions:
Several encoder wheels were sent for analysis. The samples are described below. (more…)

Bacillus globigii spores in terbium reagent

Tuesday, February 9th, 2010

Goal:
Illustrate the effect of the variable delay microcode on the shape of the terbium spectrum (more…)

LIBS Analysis of Materials Generated During the Zinc Refinement Process

Tuesday, February 9th, 2010

Goal:
Assess the feasibility of using LIBS to detect various elements in materials generated during the zinc refinement process (more…)

Non-intrusive Reflective pH Sensing in Tubes of Muddied/Sediment Water

Friday, January 15th, 2010

Goal
There was an interest in non-intrusively monitoring pH in tubes containing wet soil samples. This was significant for a number of reasons; this was the first time the reflective patches were to be tested in something other than a cuvette, on a curved surface rather, and this was also the first time an analyte solution was observed that contained sediment or turbidity. (more…)

Measuring Headspace of Organic Solvents

Friday, January 15th, 2010

Abstract
This application note explains how oxygen concentration is measured in the headspace of organic solvents such as Acetonitrile. (more…)

Smart Oxygen Cuvette for Optical Monitoring of Dissolved Oxygen in Biological Blood Samples

Tuesday, January 12th, 2010

A smart Oxygen Cuvette is developed by coating the inner surface of a cuvette with oxygen sensitive thin film material. The coating is glass like sol-gel based sensor that has an embedded ruthenium compound in the glass film. The fluorescence of the ruthenium is quenched depending on the oxygen level. Ocean Optics phase fluorometer, NeoFox is used to measure this rate of fluorescence quenching and computes it for the amount of oxygen present. (more…)

HiOXY Measurement of Methane Gas

Monday, December 28th, 2009

Goal:
To measure oxygen for the purpose of detecting methane gas. (more…)

Measuring Oxygen Concentration in Headspace

Wednesday, December 9th, 2009

Goal:

To measure oxygen concentration is measured in the headspace of organic solvents such as Acetonitrile) using a phase fluorometer system (more…)

PNNL pH Sediment Tubes

Tuesday, December 8th, 2009

Goal:
Non-intrusive Reflective pH Sensing in Tubes of Muddied/Sediment Water (more…)

Effect of fiber diameter on fluorescein fluorescence

Monday, October 26th, 2009

Goal:
Assess the effect of various fiber diameters on fluorescein fluorescence (more…)